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1 H NMR (CD 3 OD, 400 MHz) δ 8.50 (d, J = 9.6 Hz, 1H), 8.27 (d, J = 9.6 Hz, 1H), 7.78 (d, J = 9.2 Hz, 1H), 7.65 (dd, J = 9.4, 2.6 Hz, 1H), 7.52 (d, J = 3.2 Hz, 1H), 7.25 (dd, J = 6.8, 2.0 Hz, 2H), 6.93 (dd, J = 6.6, 2.2 Hz, 2H), 4.73–4.68 (m, 1H), 3.89–3.84 (m, 1H), 3.77–3.72 (m, 1H), 3.68 (s, 3H), 3.58–3.53 (m, 1H), 3.48–3.42 (m, 1H), 3.29–3.27 (m, 1H), 3.26 (s, 3H), 3.18–3.08 (m, 4H), 2.65–2.60 (m, 1H)